in this article the theory, detection, sample injection of hsce and its application in various fields are introduced.
本文着重介绍了高速毛细管电泳技术的理论、进样方法、检测器及其在各个领域的应用。
among them, the optimization of sample injection mode, selection of preconditions for capillary column, influence of electrolysis, temperature control and signal processing are more important.
其中,进样方式优化、毛细管预处理条件的选择、电极电解作用的影响、温度控制和后期的信号处理尤为重要。
a simple sample injection technique which can he considered as a simplification of cold on-column injection has been proposed.
本文提出了一种简化的毛细管色谱「冷柱上进样」技术并对其性能进行了研究。
the condition of applied voltages for pinched sample injection was optimized.
通过实验优化了夹流式进样的电压条件。
the amounts of copper in fodder was determined by gfaas with suspension sample injection digested in advance in this paper. conditions of determination were tested.
采用预消化悬浮液进样gfaas法测定饲料样品中的铜,并对测定条件进行了较深入的研究。
direct sample injection method are adopted.
采用直接进样分析。
the effect of sds concentration, sample matrix, water injection time, sample injection time and sample injection voltage were optimized.
讨论了sds浓度、样品基体、进样电压、进水时间和进样时间对富集和分离的影响。
field-amplified sample injection in capillary electrophoresis with amperometric detection is reported. the effects of the injection mode on separation and detection are discussed.